Однозарядные аргидные ионы ArM+ в методе масс-спектрометрии с индуктивно связанной плазмой
- Авторы: Пупышев А.А.1
-
Учреждения:
- Уральский федеральный университет
- Выпуск: Том 78, № 9 (2023)
- Страницы: 783-806
- Раздел: Обзоры
- Дата подачи: 14.10.2023
- URL: https://journals.rcsi.science/0044-4502/article/view/136055
- DOI: https://doi.org/10.31857/S0044450223090116
- EDN: https://elibrary.ru/ZYAAHP
- ID: 136055
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Аннотация
Рассмотрено проявление в методе масс-спектрометрии с индуктивно связанной плазмой (МС-ИСП) однозарядных аргидных ионов ArМ+, которые могут создавать значимые спектральные помехи при определении всех элементов Периодической системы с атомным номером выше 40 и измерении их изотопного состава. Приведены примеры таких характерных помех, указаны рекомендуемые и используемые таблицы помех для различных элементов. Обобщены опубликованные данные по определению энергий диссоциации ионов ArМ+ экспериментальными и теоретическими методами. Обсуждена связь энергий диссоциации аргидных ионов с их интенсивностями в масс-спектре. Рассмотрено экспериментальное определение численных значений уровня помех ArM+/M+ в МС-ИСП и влияние различных приборных и операционных факторов на это отношение. Указаны основные пути учета, снижения интенсивности ArM+ в масс-спектрах или полного удаления помех аргидных ионов. Сделаны заключение и рекомендации по рассмотренным публикациям.
Об авторах
А. А. Пупышев
Уральский федеральный университет
Автор, ответственный за переписку.
Email: pupyshev@gmail.com
Россия, 620066, Екатеринбург, ул. Мира, 19
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