Determination of free nitrogen in carbon steels by inert gas fusion method


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Abstract

The possibility to use hot extraction (thermal extraction in a carrier-gas flow) for fractional analysis of nitrogen in carbon steels is shown for cord and reinforcing-bar steels. A rapid procedure is developed for an analysis of free nitrogen in carbon steels. The validity of the analytical procedure is confirmed by high-temperature hydrogen extraction. The data obtained by the two methods correlate well with each other. A sample preparation procedure is developed for the determination of the content of dissolved nitrogen.

About the authors

Ya. I. Tabakov

Baikov Institute of Metallurgy and Materials Science

Author for correspondence.
Email: YTabakov@gmail.com
Russian Federation, Leninskii pr. 49, Moscow, 119991

K. V. Grigorovich

Baikov Institute of Metallurgy and Materials Science

Email: YTabakov@gmail.com
Russian Federation, Leninskii pr. 49, Moscow, 119991

E. R. Mansurova

Baikov Institute of Metallurgy and Materials Science

Email: YTabakov@gmail.com
Russian Federation, Leninskii pr. 49, Moscow, 119991


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