Synthesis of Magnetite Nanoparticles upon Microwave and Convection Heating


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Abstract

Size-dependent properties of magnetite (Fe3O4) nanoparticles, obtained by convection heating and by the microwave method, are compared. Generally, the synthetic procedures involving microwave heating require less time and provide smaller particle sizes and narrower size distribution. Consequently, the specific area of the prepared samples increases. The results are based on the X-ray phase analysis, transmission electron microscopy (TEM), and nitrogen adsorption measurements (Brunauer–Emmett–Teller method).

About the authors

E. M. Kostyukhin

Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences

Author for correspondence.
Email: kostyuhin.egor@gmail.com
Russian Federation, Moscow, 119991

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