Synthesis of Magnetite Nanoparticles upon Microwave and Convection Heating
- Authors: Kostyukhin E.M.1
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Affiliations:
- Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
- Issue: Vol 92, No 12 (2018)
- Pages: 2399-2402
- Section: Physical Chemistry of Hybrid Nanomaterials and Multicomponent Systems
- URL: https://journals.rcsi.science/0036-0244/article/view/170239
- DOI: https://doi.org/10.1134/S0036024418120233
- ID: 170239
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Abstract
Size-dependent properties of magnetite (Fe3O4) nanoparticles, obtained by convection heating and by the microwave method, are compared. Generally, the synthetic procedures involving microwave heating require less time and provide smaller particle sizes and narrower size distribution. Consequently, the specific area of the prepared samples increases. The results are based on the X-ray phase analysis, transmission electron microscopy (TEM), and nitrogen adsorption measurements (Brunauer–Emmett–Teller method).
Keywords
About the authors
E. M. Kostyukhin
Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Author for correspondence.
Email: kostyuhin.egor@gmail.com
Russian Federation, Moscow, 119991
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