Synthesis, crystal and molecular structure of 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane

I. V. Grishina; D. V. Makeev; V. B. Rybakov; V. L. Lapteva; V. A. Palyulin; N. S. Zefirov

doi:10.1134/S0012500817110015

Synthesis, crystal and molecular structure of 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane

Autores: Grishina I.¹, Makeev D.¹, Rybakov V.¹, Lapteva V.¹, Palyulin V.¹, Zefirov N.¹
Afiliações:
1. Lomonosov Moscow State University
Edição: Volume 477, Nº 1 (2017)
Páginas: 239-243
Seção: Chemistry
URL: https://journals.rcsi.science/0012-5008/article/view/154089
DOI: https://doi.org/10.1134/S0012500817110015
ID: 154089

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Resumo

3,7-Ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonane has been found to adopt a chair–chair conformation in the crystalline state in contrast to 3,7-ditosyl-1,5-diphenyl-3,7-diazabicyclo[3.3.1]nonan-9-one, which had been previously found to exist in a chair-boat conformation.